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61.
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Thin films on aluminum-tungsten alloys were prepared by co-deposition of pure aluminum and pure tungsten, each sputtered by an independently controlled magnetron source, on glass and sapphire substrates. Completely amorphous films were obtained in the Al80W20-Al67W33 composition range. Passivity and corrosion behavior of amorphous Al-W alloys were investigated in 1 M deaerated hydrochloric acid solution using polarization and impedance spectroscopy measurements and have been correlated with the properties of pure alloy components. Tungsten and sputter-deposited Al-W thin films are inherently passive materials while aluminum undergoes pitting corrosion in hydrochloric acid solution. The passive film formed at the OCP on each alloy possesses excellent electric and dielectric properties comparable to those of the isolating film on tungsten. The absolute impedance increases with increasing tungsten content in the alloy. According to electrochemical polarization measurements, alloying Al with W in solid solution significantly enhances the material's resistance to pitting corrosion by shifting the breakdown potential above 2000 mV (Al67W33) and lowering the corrosion rate at the OCP by more than two orders of magnitude. The most likely mechanism explaining the passivity of amorphous Al-W alloys, the Solute Vacancy Interaction Model (SVIM), involves the formation of complexes between highly oxidized solute atoms (W+6) and mobile cation vacancies, which restrict the transport of Cl− through the oxide film and inhibit its breakdown in hydrochloric acid solution. The role that film stress relaxation effects and microscopic defects in amorphous Al-W films, of the some composition, and deposited on various substrates play in their corrosion resistance is discussed. 相似文献
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D. C. Peets R. Liang C. Stock W. J. L. Buyers Z. Tun L. Taillefer R. J. Birgeneau D. A. Bonn W. N. Hardy 《Journal of Superconductivity and Novel Magnetism》2002,15(6):531-534
We have grown cubic centimeter-size crystals of YBa2Cu3O x suitable for neutron studies, by a top-seeded melt-growth technique. Growth conditions were optimized with an eye toward maximizing phase purity. It was found that the addition of 2% Y2BaCuO5 and 0.5% Pt (by mass) were required to prevent melt loss and to obtain the highest crystallinity. A neutron diffraction study on a mosaic of six such crystals found that the final Y2BaCuO5 concentration was 5%, while other impurity phases comprised less than 1% by volume. The oxygen content was set to x = 6.5, the crystals were detwinned, and then carefully annealed to give the well-ordered ortho-II phase. The neutron study determined that 70% of the mosaic's volume was in the majority orthorhomic domain. The neutron (006) and (110) rocking curve widths were ~1° per crystal and ~2.2° for the mosaic, and the oxygen chain correlation lengths were >100 Å in the a- and b-directions and ~50 Å in the c-direction. 相似文献
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标准物质在分析测试中的重要地位及发展前景 总被引:2,自引:0,他引:2
标准物质在分析测试领域中无论在定值,方法的研究,误差确定等方面都有着重要地位。标准物质的质量保证及正确使用也应引起我们重视。随着科学技术迅速发展标准物质有着广阔发展前景。 相似文献
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J.Z. ZhaoT.S. Chen 《International Journal of Heat and Mass Transfer》2002,45(11):2265-2276
The inertia effect on the onset of thermal instability in natural convection flow over heated horizontal and inclined flat plates embedded in fluid-saturated porous media is analyzed. The linear non-parallel flow model is employed in the instability analysis, which takes into account the streamwise variation as well as the transverse variation of the disturbance amplitude functions. The set of partial differential equations for the disturbance amplitude functions are converted to a system of homogeneous linear ordinary differential equations with homogeneous boundary conditions by the local non-similarity method. The resulting eigenvalue problem is then solved by an implicit finite-difference method. Representative neutral stability curves and critical Rayleigh numbers are presented. It has been found that as the angle of inclination relative to the horizontal increases, the surface heat transfer rate increases, whereas the flow becomes more stable to the vortex mode of instability. Also, as the inertia effect, expressed in terms of Forchheimer number, Fr, increases, the heat transfer rate decreases, but the flow becomes more stable. It is demonstrated that the non-parallel flow model predicts a more stable flow than the parallel flow model. 相似文献
70.
京移通信设计院从1997年启动ISO9000质量管理体系标准贯彻落实(简称贯标)工作至今已八年多。八年来本院质量管理工作上了两个台阶。 相似文献